Capillary Electrophoresis Workshop - Day 1

Time
Topic
Instructor(s)
8:30 – 9:00 a.m. Registration  
9:00 9:15 a.m.

Welcome & Introduction

  1. Purpose of the workshop
  2. Instructors
  3. FacilitiesAgenda Review
Northrop, McDermot, Jagmin, Heegel
9:50 – 10:00 a.m. Break  
10:00 – 10:50 a.m.

Overview of CE Analysis

  1. Separation Principles
  2. Instrumentation
  3. Sample preparation methods
Northrop
10:50 11:00 a.m. Break  
11:00 – 11:50 a.m.

Overview of CE Analysis (continued)

  1. Modes of Separation
    1. Cations
    2. Anions
    3. Neutrals
    4. Chiral
    5. Dynamic coating
Northrop
12:00 – 1:00 p.m. Lunch  
1:00 -  2:00 p.m.

Overview of Methamphetamine Manufacture

  1. History
  2. Ammonia Methods
    1. One-pot method
  3. HI methods
    1. HI/Red P
    2. Hypo
    3. Phosphorous Acid
  4. Others
Northrop
2:00 – 2:15 p.m. Break  
2:45 4:30 p.m.

Ammonia Method Manufacturing with CE and GC/MS

  1. Ammonia Method of Manufacture
  2. One-pot Manufacture
    1. Lithium
      1. CE cation analysis
      2. CE anion analysis
      3. GC/MS analysis
    1. Sodium
      1. CE cation analysis
      2. CE anion analysis
      3. GC/MS analysis
Jagmin, Heegel

Go to Day 2